By Deborah Levyhamburg

Integrated in a hundred and one Double-Ended Hook are heavily woven sew styles to the extra open and lacy Crochenit™ stitches. a photo of every part of the swatch demonstrates which stitches paintings top for reversible designs. All you must be sure is whether or not to make a dishcloth, position mat, afghan or a wearable garment.

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Pratt, R. G. Rice, and R. W. Luckenbaugh, J. Am. Chem. Soc. 79, 1212 (1957). B. D. Tilak and M. S. Mathur, J. Sei. Ind. Res. (India) 17B, 33 (1958). 23 I. NAPHTHOQUINONOID DYES AND PIGMENTS I t is interesting to note t h a t whereas benzoylacetonitrile reacts with (I) in the presence of isoquinoline to yield (XLVII), the reaction when carried out in presence of pyridine does not yield a pyrrocoline derivative, but gives 2-phenyl-3-cyano[2,3-&]naphthofuran-4,9-dione (XLVIII). 3 3 2. Synthesis of 2,3-Phthaloylpyrrocolines by Ring Closure of Ylidene-enol Betaines Methylation of the pyridinium betainę (XX) with dimethyl sulfate yields 3-(2-methoxy-l ,4-naphthoquinonyl)pyridinium methosulfate (XLIX).

69 C. NAPHTHOTHIAZOLEDIONES Condensation of 2-amino-3-mercapto-l ,4-naphthoquinone (CXX) with formaldehyde yields naphthothiazoledione (CXXI). 7 1 , 7 2 Substituted naphthothiazolediones are obtained by condensing (CXX) with other aldehydes such as glyoxal, acetaldehyde, benzaldehyde, and dimethylaminobenzaldehyde. When dialdehydes such as terephthaldehyde are condensed with (CXX), bis naphthothiazolediones of the type (CXXII) are formed. Bis naphthothiazolediones dye cotton from an alkaline hydrosulfite bath, giving yellow shades.

Boyle, J. Org. Chem. 24, 374 (1959). 36 B. D. TIL AK pyridine in 2-ethoxyethanol. 66 The mechanism of formation of (XCI) by the latter route is shown below. Various substituted 2-aminopyridines, such as methyl, chloro, ethoxy, 5-nitro, and 3,5-dinitro-2-aminopyridines have been used in this reaction to yield a series of naphthimidazopyridinediones with substituents in the pyridine ring. Derivatives of (I) containing nitro, halo, and hydroxy substituents have also been used in the reaction to give derivatives of (XCI) which have been reported as useful vat dyes and pigments.

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